Science Journal of Analytical Chemistry

Volume 8, Issue 1, March 2020

  • An Analytical Procedure by the Inductively Coupled Plasma Mass Spectrometry (ICP-MS) for the Quantitation of Total Phosphorus Content on the Surface of the Manufacturing Equipment for Oligonucleotides

    Daisuke Furukawa, Masami Nakai, Masato Kazusaki

    Issue: Volume 8, Issue 1, March 2020
    Pages: 1-4
    Received: 25 December 2019
    Accepted: 07 January 2020
    Published: 30 January 2020
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    Abstract: An analytical procedure by the inductively coupled plasma mass spectrometry (ICP-MS) is provided to quantitate the remaining phosphorus amount on the surface of the manufacturing equipment for the oligonucleotide active pharmaceutical ingredient (API). In this analytical procedure, the sample solutions obtained from the rinse sampling and direct su... Show More
  • Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar

    Qiang Sun, Yuliang Gao, Liyan Wang

    Issue: Volume 8, Issue 1, March 2020
    Pages: 5-11
    Received: 21 December 2019
    Accepted: 08 January 2020
    Published: 31 January 2020
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    Abstract: A simple, efficient and environmentally friendly method has been established for the analysis of organic components in wood vinegar (WV) by dispersive liquid-liquid micro-extraction based on solidification of floating organic droplet (DLLME-SFO) coupled with GC/MS. Several variables that affect the extraction efficiency, including the type and volu... Show More
  • LC/MS Analysis of Cyclo Fatty Acid-containing Triacylglycerols in Cottonseed Oil

    Shuji Hirayama, Daichi Shinozaki, Yoshiya Izumi

    Issue: Volume 8, Issue 1, March 2020
    Pages: 12-17
    Received: 22 December 2019
    Accepted: 15 January 2020
    Published: 31 January 2020
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    Abstract: We measured the constituent triacylglycerol of cotton oil, the only edible oil containing a cyclo fatty acid. Due to the difficulty of obtaining a standard for triacylglycerols containing cyclo fatty acids, cotton oil is analyzed using cyclo triacylglycerol in kapok oil as a reference. Analytical methods used liquid chromatography fast atom bombard... Show More
  • Fatty Amides in Minutes: Direct Formation from Fatty Esters in a Green Synthetic Process

    Onyanobi Abel-Anyebe, Nabil Idris, Djene Keita, Kieran Ita Ekpenyong, Momoh Audu Yakubu

    Issue: Volume 8, Issue 1, March 2020
    Pages: 18-28
    Received: 25 July 2019
    Accepted: 20 August 2019
    Published: 13 February 2020
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    Abstract: Fatty amides are used in the manufacture of drugs, cosmetics, plastics, insecticides, etc. but the synthetic process involves fatty ester-derived fatty acid steps with economic and environmental consequences. Fatty esters (vegetable oils) are available in abundance and renewable but have not been used directly or cost effectively in the production ... Show More
  • Glycemic Index of Traditional Meal (Dambu) from Pearl Millet and Maize

    Maimuna Ladidi Aliyu, Safiya Aliyu Tijjani, Danladi Amodu Ameh, Aisha Babagana

    Issue: Volume 8, Issue 1, March 2020
    Pages: 29-32
    Received: 13 February 2020
    Accepted: 25 February 2020
    Published: 10 March 2020
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    Abstract: The aim of this study is to determine the blood glucose response of traditionally prepared meal called Dambu from millet and maize enriched with beans, groundnut and vegetables. The cereals grains and other ingredients were purchased from a local market in Kaduna metropolis, and the preparation of the meal, blood glucose response with glycemic inde... Show More
  • Standardisation Process of Saye, a Traditional Polyherbal Formulation Remedy for Malaria: Physico-chemical Analysis and Phytochemical Investigation

    Jules Yoda, Jean Claude Ouedraogo, Salfo Ouedraogo, Maminata Traore-Coulibaly, Felix Kini, Marius Lompo, Sylvin Ouedraogo

    Issue: Volume 8, Issue 1, March 2020
    Pages: 33-40
    Received: 18 February 2020
    Accepted: 03 March 2020
    Published: 10 March 2020
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    Abstract: The use of herbal drugs for primary care is nowadays central to the global health system. In developing countries, it meets both economic and socio-cultural requirements. However, this increase about the use of herbal medicines has led to various forms of abuses related to factors that are generally extrinsic to the drug, such as incorrect botanica... Show More