Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath

Dhananjay kumar Singh; Manoj Kumar Tripathi; V. B. Singh

doi:doi:10.11648/j.ijmsa.20130202.16

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Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath

Dhananjay kumar Singh, Manoj Kumar Tripathi, V. B. Singh

Received: 14 February 2013 Accepted: Published: 10 January 2013

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Abstract

Composite coating of tungsten carbide (WC) in the matrix of nickel has been achieved by direct current (DC) electrodeposition technique using a non aqueous bath. The deposition parameters such as current density, bath temperature, and stirring rate were maintained at constant levels for all the coating configurations. The composition of the coating and its microstructure were studied using energy dispersive x-ray spectroscopy, uv-vis spectrophotometry and x-ray diffraction, respectively. Surface morphology of the coatings was studied by scanning electron microscopy (SEM and TEM). Effect of heat treatment on the deposits microstructures and microhardness was also investigated. The Ni–WC composites, prepared at optimum conditions, exhibited improved mechanical properties in comparison to pure nickel electrodeposits.

DOI	10.11648/j.ijmsa.20130202.16
Published in	International Journal of Materials Science and Applications (Volume 2, Issue 2, March 2013)
Page(s)	68-73
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Electrodeposition, Ni-WC composite, Microhardness, Microstructure

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APA Style

Dhananjay kumar Singh, Manoj Kumar Tripathi, V. B. Singh. (2013). Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath. International Journal of Materials Science and Applications, 2(2), 68-73. https://doi.org/10.11648/j.ijmsa.20130202.16

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ACS Style

Dhananjay kumar Singh; Manoj Kumar Tripathi; V. B. Singh. Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath. Int. J. Mater. Sci. Appl. 2013, 2(2), 68-73. doi: 10.11648/j.ijmsa.20130202.16

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AMA Style

Dhananjay kumar Singh, Manoj Kumar Tripathi, V. B. Singh. Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath. Int J Mater Sci Appl. 2013;2(2):68-73. doi: 10.11648/j.ijmsa.20130202.16

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@article{10.11648/j.ijmsa.20130202.16,
  author = {Dhananjay kumar Singh and Manoj Kumar Tripathi and V. B. Singh},
  title = {Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath},
  journal = {International Journal of Materials Science and Applications},
  volume = {2},
  number = {2},
  pages = {68-73},
  doi = {10.11648/j.ijmsa.20130202.16},
  url = {https://doi.org/10.11648/j.ijmsa.20130202.16},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20130202.16},
  abstract = {Composite coating of tungsten carbide (WC) in the matrix of nickel has been achieved by direct current (DC) electrodeposition technique using a non aqueous bath. The deposition parameters such as current density, bath temperature, and stirring rate were maintained at constant levels for all the coating configurations. The composition of the coating and its microstructure were studied using energy dispersive x-ray spectroscopy, uv-vis spectrophotometry and x-ray diffraction, respectively. Surface morphology of the coatings was studied by scanning electron microscopy (SEM and TEM). Effect of heat treatment on the deposits microstructures and microhardness was also investigated. The Ni–WC composites, prepared at optimum conditions, exhibited improved mechanical properties in comparison to pure nickel electrodeposits.},
 year = {2013}
}

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TY  - JOUR
T1  - Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath
AU  - Dhananjay kumar Singh
AU  - Manoj Kumar Tripathi
AU  - V. B. Singh
Y1  - 2013/01/10
PY  - 2013
N1  - https://doi.org/10.11648/j.ijmsa.20130202.16
DO  - 10.11648/j.ijmsa.20130202.16
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 68
EP  - 73
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20130202.16
AB  - Composite coating of tungsten carbide (WC) in the matrix of nickel has been achieved by direct current (DC) electrodeposition technique using a non aqueous bath. The deposition parameters such as current density, bath temperature, and stirring rate were maintained at constant levels for all the coating configurations. The composition of the coating and its microstructure were studied using energy dispersive x-ray spectroscopy, uv-vis spectrophotometry and x-ray diffraction, respectively. Surface morphology of the coatings was studied by scanning electron microscopy (SEM and TEM). Effect of heat treatment on the deposits microstructures and microhardness was also investigated. The Ni–WC composites, prepared at optimum conditions, exhibited improved mechanical properties in comparison to pure nickel electrodeposits.
VL  - 2
IS  - 2
ER  -

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Author Information

Dhananjay kumar Singh

Department of chemistry, Faculty of Science, Banaras Hindu University, Varanasi-221005, India
Manoj Kumar Tripathi

Department of chemistry, Faculty of Science, Banaras Hindu University, Varanasi-221005, India
V. B. Singh

Department of chemistry, Faculty of Science, Banaras Hindu University, Varanasi-221005, India

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APA Style

Dhananjay kumar Singh, Manoj Kumar Tripathi, V. B. Singh. (2013). Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath. International Journal of Materials Science and Applications, 2(2), 68-73. https://doi.org/10.11648/j.ijmsa.20130202.16

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ACS Style

Dhananjay kumar Singh; Manoj Kumar Tripathi; V. B. Singh. Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath. Int. J. Mater. Sci. Appl. 2013, 2(2), 68-73. doi: 10.11648/j.ijmsa.20130202.16

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AMA Style

Dhananjay kumar Singh, Manoj Kumar Tripathi, V. B. Singh. Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath. Int J Mater Sci Appl. 2013;2(2):68-73. doi: 10.11648/j.ijmsa.20130202.16

Copy | Download

@article{10.11648/j.ijmsa.20130202.16,
  author = {Dhananjay kumar Singh and Manoj Kumar Tripathi and V. B. Singh},
  title = {Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath},
  journal = {International Journal of Materials Science and Applications},
  volume = {2},
  number = {2},
  pages = {68-73},
  doi = {10.11648/j.ijmsa.20130202.16},
  url = {https://doi.org/10.11648/j.ijmsa.20130202.16},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20130202.16},
  abstract = {Composite coating of tungsten carbide (WC) in the matrix of nickel has been achieved by direct current (DC) electrodeposition technique using a non aqueous bath. The deposition parameters such as current density, bath temperature, and stirring rate were maintained at constant levels for all the coating configurations. The composition of the coating and its microstructure were studied using energy dispersive x-ray spectroscopy, uv-vis spectrophotometry and x-ray diffraction, respectively. Surface morphology of the coatings was studied by scanning electron microscopy (SEM and TEM). Effect of heat treatment on the deposits microstructures and microhardness was also investigated. The Ni–WC composites, prepared at optimum conditions, exhibited improved mechanical properties in comparison to pure nickel electrodeposits.},
 year = {2013}
}

Copy | Download

TY  - JOUR
T1  - Electrocodeposition and Characterization of Ni-WC Composite Coating From Non – Aqueous Bath
AU  - Dhananjay kumar Singh
AU  - Manoj Kumar Tripathi
AU  - V. B. Singh
Y1  - 2013/01/10
PY  - 2013
N1  - https://doi.org/10.11648/j.ijmsa.20130202.16
DO  - 10.11648/j.ijmsa.20130202.16
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 68
EP  - 73
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20130202.16
AB  - Composite coating of tungsten carbide (WC) in the matrix of nickel has been achieved by direct current (DC) electrodeposition technique using a non aqueous bath. The deposition parameters such as current density, bath temperature, and stirring rate were maintained at constant levels for all the coating configurations. The composition of the coating and its microstructure were studied using energy dispersive x-ray spectroscopy, uv-vis spectrophotometry and x-ray diffraction, respectively. Surface morphology of the coatings was studied by scanning electron microscopy (SEM and TEM). Effect of heat treatment on the deposits microstructures and microhardness was also investigated. The Ni–WC composites, prepared at optimum conditions, exhibited improved mechanical properties in comparison to pure nickel electrodeposits.
VL  - 2
IS  - 2
ER  -

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