Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer

Yasuyoshi Fukui; Daisaku Nara; Kazuyo Fushimi; Noriyoshi Kumazawa

doi:doi:10.11648/j.ijmsa.20140306.21

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Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer

Yasuyoshi Fukui, Daisaku Nara, Kazuyo Fushimi, Noriyoshi Kumazawa

Published in International Journal of Materials Science and Applications (Volume 3, Issue 6)

Received: 22 October 2014 Accepted: 6 November 2014 Published: 20 November 2014

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Abstract

This paper presents of studies performed to assess the effect of rheological behavior on the near-net shape forming of an Al–20 vol% SiC composite of Duralcan F3A.20S and of the mother aluminum alloy A356 for comparison. Isothermal experiments were conducted using results of a parallel-plate drop-forge viscometer in a temperature range from 849 K (576 ºC) to 862 K (590 ºC). Each experiment indicated that the viscosity decreased in the early increasing shear rate stage and subsequently increased with decreasing shear rate. The overall relationship between the viscosity,μ[Pa.s], and the shear rate,γ[s-1], can be described by a power-law model of μ= 3.2 × 107γ-1.5 for Duralcan and μ = 1.6 × 107γ-1.5 for A356. The power-law index was the same for both materials, whereas the power-law constant of Duralcan was two times greater than that of the A356 mother alloy because of the distribution of 20 vol% SiC particles. The decrease in the viscosity that accompanied an increase in the shear rate depended on both the temperature and the applied force. The viscosities of 32 kPa.s for both Duralcan and A356 at the maximum effective duration of deformation, which obtained from the plot as a function of the viscosity, appeared to be the points at which the dominant factor governing the visco-plastic flow process transitions from plastic forming to casting. The viscosity must also represent optimum semi-solid forming conditions, as indicated by the achievement of both a moderate working time and an adequate deformation. The optimum operating temperature for both materials can be ranged from 855 K (582 ˚C) to 857 K (584 ˚C), which is just above the melting point.

Published in	International Journal of Materials Science and Applications (Volume 3, Issue 6)
DOI	10.11648/j.ijmsa.20140306.21
Page(s)	344-352
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Semi-Solid Forming, Composite Material, Rheology, Visco-Plastic Flow

References

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[2]	J.U. Ejiofor, and R.G.Reddy, “Developments in the processing and properties of particulate Al-Si composites”, JOM, Vol. 49, No. 11, pp. 31-37, 1997.
[3]	V. Laxmanan and M.C. Flemings, “Deformation of Semi-Solid Sn-15 Pct Pb Alloy”, Metallurgical Transactions A, Vol.11A, No.12, pp. 1927-1937, 1980.
[4]	P.J. Ward, H.V. Atkinson, P.R.G. Anderson, L.G. Elias, B. Garcia, L. Kahlen, and J-M. Rodrigues-Ibabe, “Semi-Solid Processing of Novel MMCs Based on Hypereutectic Aluminum-Silicon Alloys”, Acta Metallurgica et Materialia, Vol.44, No.5, pp. 1717-1727, 1996.
[5]	H. Iwasaki, T. Mori, M. Mabuchi, and K. Higashi, “Shear Deformation Behavior of Al-5% Mg in a Semi-Solid State”, Acta Metallurgica et Materialia, Vol.46, No.18, pp. 6351-6360, 1998.
[6]	J.A. Yurko and M.C. Flemings, “Rheology and Microstructure of Semi-Solid Aluminum Alloys Compressed in the Drop Forge Viscometer”, Metallurgical and Materials Transactions A, Vol.33A, No.8, pp. 2737-2746, 2002.
[7]	K. Solek, Z. Mitura, R. Kuzaik, and P. Kapranos, “The use of ADINA software to simulate thixocasting processes”, Solid State Phenomena, Vols. 116-117, pp. 626-629, 2006.
[8]	Y. Fukui, H. Okada, N. Kumazawa, and Y. Watanabe, “Near Net Shape Forming of Al-Al3Ni FGM over Eutectic Melting Temperature”, Metallurgical and Materials Transactions A, Vol. 31A, No. 10, pp. 2627-2636, 2000.
[9]	K. Yamagiwa, Y. Watanabe, K. Matsuda, Y. Fukui, and P. Kapranos, “Characteristic of Al-Al3Fe Eco-Functionally Graded Material through Near-Net-Shape Forming over Eutectic Melting Temperature”, Materials Science and Engineering A, Vol. A416, Nos. 1-2, pp. 80-91, 2006.
[10]	M.C. Flemings, “Behavior of Metal Alloys in the Semisolid State”, Metallurgical Transactions A, Vol.22A, No.5, pp. 957-981, 1991.
[11]	D.H. Kirkwood, “Semisolid metal processing”, International Materials Reviews,Vol.39, pp. 173-189, 1994.
[12]	G.J. Dienes and H.F. Klemm, “Theory and Application of the Parallel Plate Plastometer”, Journal of Applied Physics, Vol.17, pp. 458-471, 1946.
[13]	J.V. Robinson, “The Viscosity of Suspensions of Spheres”, The Journal of Physical Chemistry, Vol.53, No.7, pp. 1042-1056, 1949.
[14]	M. Mooney, “The viscosity of a concentrated suspension of spherical particles”, Journal of Colloid Science, Vol.6, pp. 162-170, 1951.

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Yasuyoshi Fukui, Daisaku Nara, Kazuyo Fushimi, Noriyoshi Kumazawa. (2014). Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer. International Journal of Materials Science and Applications, 3(6), 344-352. https://doi.org/10.11648/j.ijmsa.20140306.21

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ACS Style

Yasuyoshi Fukui; Daisaku Nara; Kazuyo Fushimi; Noriyoshi Kumazawa. Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer. Int. J. Mater. Sci. Appl. 2014, 3(6), 344-352. doi: 10.11648/j.ijmsa.20140306.21

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AMA Style

Yasuyoshi Fukui, Daisaku Nara, Kazuyo Fushimi, Noriyoshi Kumazawa. Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer. Int J Mater Sci Appl. 2014;3(6):344-352. doi: 10.11648/j.ijmsa.20140306.21

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@article{10.11648/j.ijmsa.20140306.21,
  author = {Yasuyoshi Fukui and Daisaku Nara and Kazuyo Fushimi and Noriyoshi Kumazawa},
  title = {Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer},
  journal = {International Journal of Materials Science and Applications},
  volume = {3},
  number = {6},
  pages = {344-352},
  doi = {10.11648/j.ijmsa.20140306.21},
  url = {https://doi.org/10.11648/j.ijmsa.20140306.21},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20140306.21},
  abstract = {This paper presents of studies performed to assess the effect of rheological behavior on the near-net shape forming of an Al–20 vol% SiC composite of Duralcan F3A.20S and of the mother aluminum alloy A356 for comparison. Isothermal experiments were conducted using results of a parallel-plate drop-forge viscometer in a temperature range from 849 K (576 ºC) to 862 K (590 ºC). Each experiment indicated that the viscosity decreased in the early increasing shear rate stage and subsequently increased with decreasing shear rate. The overall relationship between the viscosity,μ[Pa.s], and the shear rate,γ[s-1], can be described by a power-law model of μ= 3.2 × 107γ-1.5 for Duralcan and μ = 1.6 × 107γ-1.5 for A356. The power-law index was the same for both materials, whereas the power-law constant of Duralcan was two times greater than that of the A356 mother alloy because of the distribution of 20 vol% SiC particles. The decrease in the viscosity that accompanied an increase in the shear rate depended on both the temperature and the applied force. The viscosities of 32 kPa.s for both Duralcan and A356 at the maximum effective duration of deformation, which obtained from the plot as a function of the viscosity, appeared to be the points at which the dominant factor governing the visco-plastic flow process transitions from plastic forming to casting. The viscosity must also represent optimum semi-solid forming conditions, as indicated by the achievement of both a moderate working time and an adequate deformation. The optimum operating temperature for both materials can be ranged from 855 K (582 ˚C) to 857 K (584 ˚C), which is just above the melting point.},
 year = {2014}
}

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TY  - JOUR
T1  - Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer
AU  - Yasuyoshi Fukui
AU  - Daisaku Nara
AU  - Kazuyo Fushimi
AU  - Noriyoshi Kumazawa
Y1  - 2014/11/20
PY  - 2014
N1  - https://doi.org/10.11648/j.ijmsa.20140306.21
DO  - 10.11648/j.ijmsa.20140306.21
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 344
EP  - 352
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20140306.21
AB  - This paper presents of studies performed to assess the effect of rheological behavior on the near-net shape forming of an Al–20 vol% SiC composite of Duralcan F3A.20S and of the mother aluminum alloy A356 for comparison. Isothermal experiments were conducted using results of a parallel-plate drop-forge viscometer in a temperature range from 849 K (576 ºC) to 862 K (590 ºC). Each experiment indicated that the viscosity decreased in the early increasing shear rate stage and subsequently increased with decreasing shear rate. The overall relationship between the viscosity,μ[Pa.s], and the shear rate,γ[s-1], can be described by a power-law model of μ= 3.2 × 107γ-1.5 for Duralcan and μ = 1.6 × 107γ-1.5 for A356. The power-law index was the same for both materials, whereas the power-law constant of Duralcan was two times greater than that of the A356 mother alloy because of the distribution of 20 vol% SiC particles. The decrease in the viscosity that accompanied an increase in the shear rate depended on both the temperature and the applied force. The viscosities of 32 kPa.s for both Duralcan and A356 at the maximum effective duration of deformation, which obtained from the plot as a function of the viscosity, appeared to be the points at which the dominant factor governing the visco-plastic flow process transitions from plastic forming to casting. The viscosity must also represent optimum semi-solid forming conditions, as indicated by the achievement of both a moderate working time and an adequate deformation. The optimum operating temperature for both materials can be ranged from 855 K (582 ˚C) to 857 K (584 ˚C), which is just above the melting point.
VL  - 3
IS  - 6
ER  -

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Author Information

Yasuyoshi Fukui

Graduate School of Science and Engineering, Kagoshima University, Kagoshima, Japan
Daisaku Nara

Graduate School of Science and Engineering, Kagoshima University, Kagoshima, Japan
Kazuyo Fushimi

Graduate School of Science and Engineering, Kagoshima University, Kagoshima, Japan
Noriyoshi Kumazawa

Graduate School of Science and Engineering, Kagoshima University, Kagoshima, Japan

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APA Style

Yasuyoshi Fukui, Daisaku Nara, Kazuyo Fushimi, Noriyoshi Kumazawa. (2014). Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer. International Journal of Materials Science and Applications, 3(6), 344-352. https://doi.org/10.11648/j.ijmsa.20140306.21

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ACS Style

Yasuyoshi Fukui; Daisaku Nara; Kazuyo Fushimi; Noriyoshi Kumazawa. Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer. Int. J. Mater. Sci. Appl. 2014, 3(6), 344-352. doi: 10.11648/j.ijmsa.20140306.21

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AMA Style

Yasuyoshi Fukui, Daisaku Nara, Kazuyo Fushimi, Noriyoshi Kumazawa. Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer. Int J Mater Sci Appl. 2014;3(6):344-352. doi: 10.11648/j.ijmsa.20140306.21

Copy | Download

@article{10.11648/j.ijmsa.20140306.21,
  author = {Yasuyoshi Fukui and Daisaku Nara and Kazuyo Fushimi and Noriyoshi Kumazawa},
  title = {Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer},
  journal = {International Journal of Materials Science and Applications},
  volume = {3},
  number = {6},
  pages = {344-352},
  doi = {10.11648/j.ijmsa.20140306.21},
  url = {https://doi.org/10.11648/j.ijmsa.20140306.21},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20140306.21},
  abstract = {This paper presents of studies performed to assess the effect of rheological behavior on the near-net shape forming of an Al–20 vol% SiC composite of Duralcan F3A.20S and of the mother aluminum alloy A356 for comparison. Isothermal experiments were conducted using results of a parallel-plate drop-forge viscometer in a temperature range from 849 K (576 ºC) to 862 K (590 ºC). Each experiment indicated that the viscosity decreased in the early increasing shear rate stage and subsequently increased with decreasing shear rate. The overall relationship between the viscosity,μ[Pa.s], and the shear rate,γ[s-1], can be described by a power-law model of μ= 3.2 × 107γ-1.5 for Duralcan and μ = 1.6 × 107γ-1.5 for A356. The power-law index was the same for both materials, whereas the power-law constant of Duralcan was two times greater than that of the A356 mother alloy because of the distribution of 20 vol% SiC particles. The decrease in the viscosity that accompanied an increase in the shear rate depended on both the temperature and the applied force. The viscosities of 32 kPa.s for both Duralcan and A356 at the maximum effective duration of deformation, which obtained from the plot as a function of the viscosity, appeared to be the points at which the dominant factor governing the visco-plastic flow process transitions from plastic forming to casting. The viscosity must also represent optimum semi-solid forming conditions, as indicated by the achievement of both a moderate working time and an adequate deformation. The optimum operating temperature for both materials can be ranged from 855 K (582 ˚C) to 857 K (584 ˚C), which is just above the melting point.},
 year = {2014}
}

Copy | Download

TY  - JOUR
T1  - Evaluation of the Rheological Behavior of a Semi-Solid Al–SiC Composite using a Parallel-Plate Drop-Forge Viscometer
AU  - Yasuyoshi Fukui
AU  - Daisaku Nara
AU  - Kazuyo Fushimi
AU  - Noriyoshi Kumazawa
Y1  - 2014/11/20
PY  - 2014
N1  - https://doi.org/10.11648/j.ijmsa.20140306.21
DO  - 10.11648/j.ijmsa.20140306.21
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 344
EP  - 352
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20140306.21
AB  - This paper presents of studies performed to assess the effect of rheological behavior on the near-net shape forming of an Al–20 vol% SiC composite of Duralcan F3A.20S and of the mother aluminum alloy A356 for comparison. Isothermal experiments were conducted using results of a parallel-plate drop-forge viscometer in a temperature range from 849 K (576 ºC) to 862 K (590 ºC). Each experiment indicated that the viscosity decreased in the early increasing shear rate stage and subsequently increased with decreasing shear rate. The overall relationship between the viscosity,μ[Pa.s], and the shear rate,γ[s-1], can be described by a power-law model of μ= 3.2 × 107γ-1.5 for Duralcan and μ = 1.6 × 107γ-1.5 for A356. The power-law index was the same for both materials, whereas the power-law constant of Duralcan was two times greater than that of the A356 mother alloy because of the distribution of 20 vol% SiC particles. The decrease in the viscosity that accompanied an increase in the shear rate depended on both the temperature and the applied force. The viscosities of 32 kPa.s for both Duralcan and A356 at the maximum effective duration of deformation, which obtained from the plot as a function of the viscosity, appeared to be the points at which the dominant factor governing the visco-plastic flow process transitions from plastic forming to casting. The viscosity must also represent optimum semi-solid forming conditions, as indicated by the achievement of both a moderate working time and an adequate deformation. The optimum operating temperature for both materials can be ranged from 855 K (582 ˚C) to 857 K (584 ˚C), which is just above the melting point.
VL  - 3
IS  - 6
ER  -

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