International Journal of Materials Science and Applications

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Corrosion of Heat Treated Electroless-Ni Plated Mild Carbon Steels in Dilute H2SO4

Received: 05 August 2015    Accepted: 14 August 2015    Published: 16 October 2015
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Abstract

The corrosion of heat-treated Electroless-Nickel (EN) plated mild carbon steel (MCS) in dilute H2SO4 is investigated and reported in the study. The MCS samples were electroless-Ni plated in alkaline Nimudeen 850. EN plated samples were soaked at different selected temperatures between 150-370 °C at constant time. The weight loss of the specimens by full immersion method was employed to assess the corrosion damage and corrosion rates of the as-received, EN plated MCS and four heat treated EN plated samples in the 0.5 M H2SO4 solution. The test specimens were regularly examined at every 12 hrs interval for 30 days (720 hrs). The materials corrodes in 0.5 M H2SO4 in the order of MCS10 > MCS14 > MCS15 > MCS11 > MCS13 > MCS12. Based on the results obtained, it will be justified to choose EN-plated samples (MCS 11) and the heat treated EN film (MCS12 and MCS13) for the purposed of solving the problem of corrosion in the medium. This is because; the application of EN deposition reduced the corrosion of MCS at much lower rate than the heat-treated EN film (MCS14 and MCS15) in 0.5 M H2SO4 environment. Atomic Absorption Spectrometer (AAS) Thermo series 2000 model and Scanning Electron Microscopy (SEM) with the Energy Dispersive X-Ray (EDX) facilities (Jeol JSM-7600F model) were used to ascertain the chemical compositions and the microstructures of samples.

DOI 10.11648/j.ijmsa.20150405.18
Published in International Journal of Materials Science and Applications (Volume 4, Issue 5, September 2015)
Page(s) 333-342
Creative Commons

This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Corrosion, Heat Treatment, Electroless-Ni Plating, Mild Carbon Steel, Protective EN Film

References
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Author Information
  • Department of Metallurgical and Materials Engineering, Federal University of Technology, Akure, Nigeria; Department of Materials and Metallurgical Engineering, Federal University Oye Ekiti, Oye Ekiti, Nigeria

  • Department of Materials and Metallurgical Engineering, Federal University Oye Ekiti, Oye Ekiti, Nigeria

  • Department of Metallurgical and Materials Engineering, Federal University of Technology, Akure, Nigeria

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  • APA Style

    Olawale Olarewaju Ajibola, Abdullahi O. Adebayo, Daniel Toyin Oloruntoba. (2015). Corrosion of Heat Treated Electroless-Ni Plated Mild Carbon Steels in Dilute H2SO4. International Journal of Materials Science and Applications, 4(5), 333-342. https://doi.org/10.11648/j.ijmsa.20150405.18

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    Olawale Olarewaju Ajibola; Abdullahi O. Adebayo; Daniel Toyin Oloruntoba. Corrosion of Heat Treated Electroless-Ni Plated Mild Carbon Steels in Dilute H2SO4. Int. J. Mater. Sci. Appl. 2015, 4(5), 333-342. doi: 10.11648/j.ijmsa.20150405.18

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    AMA Style

    Olawale Olarewaju Ajibola, Abdullahi O. Adebayo, Daniel Toyin Oloruntoba. Corrosion of Heat Treated Electroless-Ni Plated Mild Carbon Steels in Dilute H2SO4. Int J Mater Sci Appl. 2015;4(5):333-342. doi: 10.11648/j.ijmsa.20150405.18

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  • @article{10.11648/j.ijmsa.20150405.18,
      author = {Olawale Olarewaju Ajibola and Abdullahi O. Adebayo and Daniel Toyin Oloruntoba},
      title = {Corrosion of Heat Treated Electroless-Ni Plated Mild Carbon Steels in Dilute H2SO4},
      journal = {International Journal of Materials Science and Applications},
      volume = {4},
      number = {5},
      pages = {333-342},
      doi = {10.11648/j.ijmsa.20150405.18},
      url = {https://doi.org/10.11648/j.ijmsa.20150405.18},
      eprint = {https://download.sciencepg.com/pdf/10.11648.j.ijmsa.20150405.18},
      abstract = {The corrosion of heat-treated Electroless-Nickel (EN) plated mild carbon steel (MCS) in dilute H2SO4 is investigated and reported in the study. The MCS samples were electroless-Ni plated in alkaline Nimudeen 850. EN plated samples were soaked at different selected temperatures between 150-370 °C at constant time. The weight loss of the specimens by full immersion method was employed to assess the corrosion damage and corrosion rates of the as-received, EN plated MCS and four heat treated EN plated samples in the 0.5 M H2SO4 solution. The test specimens were regularly examined at every 12 hrs interval for 30 days (720 hrs). The materials corrodes in 0.5 M H2SO4 in the order of MCS10 > MCS14 > MCS15 > MCS11 > MCS13 > MCS12. Based on the results obtained, it will be justified to choose EN-plated samples (MCS 11) and the heat treated EN film (MCS12 and MCS13) for the purposed of solving the problem of corrosion in the medium. This is because; the application of EN deposition reduced the corrosion of MCS at much lower rate than the heat-treated EN film (MCS14 and MCS15) in 0.5 M H2SO4 environment. Atomic Absorption Spectrometer (AAS) Thermo series 2000 model and Scanning Electron Microscopy (SEM) with the Energy Dispersive X-Ray (EDX) facilities (Jeol JSM-7600F model) were used to ascertain the chemical compositions and the microstructures of samples.},
     year = {2015}
    }
    

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  • TY  - JOUR
    T1  - Corrosion of Heat Treated Electroless-Ni Plated Mild Carbon Steels in Dilute H2SO4
    AU  - Olawale Olarewaju Ajibola
    AU  - Abdullahi O. Adebayo
    AU  - Daniel Toyin Oloruntoba
    Y1  - 2015/10/16
    PY  - 2015
    N1  - https://doi.org/10.11648/j.ijmsa.20150405.18
    DO  - 10.11648/j.ijmsa.20150405.18
    T2  - International Journal of Materials Science and Applications
    JF  - International Journal of Materials Science and Applications
    JO  - International Journal of Materials Science and Applications
    SP  - 333
    EP  - 342
    PB  - Science Publishing Group
    SN  - 2327-2643
    UR  - https://doi.org/10.11648/j.ijmsa.20150405.18
    AB  - The corrosion of heat-treated Electroless-Nickel (EN) plated mild carbon steel (MCS) in dilute H2SO4 is investigated and reported in the study. The MCS samples were electroless-Ni plated in alkaline Nimudeen 850. EN plated samples were soaked at different selected temperatures between 150-370 °C at constant time. The weight loss of the specimens by full immersion method was employed to assess the corrosion damage and corrosion rates of the as-received, EN plated MCS and four heat treated EN plated samples in the 0.5 M H2SO4 solution. The test specimens were regularly examined at every 12 hrs interval for 30 days (720 hrs). The materials corrodes in 0.5 M H2SO4 in the order of MCS10 > MCS14 > MCS15 > MCS11 > MCS13 > MCS12. Based on the results obtained, it will be justified to choose EN-plated samples (MCS 11) and the heat treated EN film (MCS12 and MCS13) for the purposed of solving the problem of corrosion in the medium. This is because; the application of EN deposition reduced the corrosion of MCS at much lower rate than the heat-treated EN film (MCS14 and MCS15) in 0.5 M H2SO4 environment. Atomic Absorption Spectrometer (AAS) Thermo series 2000 model and Scanning Electron Microscopy (SEM) with the Energy Dispersive X-Ray (EDX) facilities (Jeol JSM-7600F model) were used to ascertain the chemical compositions and the microstructures of samples.
    VL  - 4
    IS  - 5
    ER  - 

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