Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat

Jie Li; Jianhuan Li; Wei Xiang; Hui Xu; Bolong Lv; Qing Wu

doi:doi:10.11648/j.sd.20190704.19

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Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat

Jie Li, Jianhuan Li, Wei Xiang, Hui Xu, Bolong Lv, Qing Wu

Published in Science Discovery (Volume 7, Issue 4)

Received: 25 June 2019 Accepted: Published: 27 August 2019

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Abstract

Aquatic animals are susceptible to N-dimethylnitrosamine pollution in water quality or feed, which is a non-negligible problem in food safety detection. Gas chromatography/triple four-stage mass spectrometry combined with QuEChERS was used to detect N-dimethylnitrosamine in duck and poultry meat, and acetonitrile, salting-out agent and purifying agent were used to extract duck and poultry meat samples. The results of detection and analysis showed that the results were good. The standard curve was highly correlated in the range of 5ng/mL to 1000ng/mL (R² > 0.9997). The recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, instrument detection limit was 4.4ng/mL and method detection limit was 0.44ng/g after adding standard sample and matrix effect treatment. The results showed that the recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, and instrument detection limit was 4 ng/mL. Other methods can reduce the operation steps and improve the detection accuracy.

Published in	Science Discovery (Volume 7, Issue 4)
DOI	10.11648/j.sd.20190704.19
Page(s)	227-231
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

N-Nitrosodimethylamine,Tiple Quadrupole Mass Spectrometer, QuEChERS, Duck Meat Products

References

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[6]	张凤艳，蒋万枫，王蓓，高嵩，桑迎迎，田玲. 水产品中N-二甲基亚硝胺气相色谱-串联质谱测定样品处理方法的改进. 中国卫生检验杂志, 2018,28 (11) ;1306-1317。
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Cite This Article

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APA Style

Jie Li, Jianhuan Li, Wei Xiang, Hui Xu, Bolong Lv, et al. (2019). Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat. Science Discovery, 7(4), 227-231. https://doi.org/10.11648/j.sd.20190704.19

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ACS Style

Jie Li; Jianhuan Li; Wei Xiang; Hui Xu; Bolong Lv, et al. Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat. Sci. Discov. 2019, 7(4), 227-231. doi: 10.11648/j.sd.20190704.19

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AMA Style

Jie Li, Jianhuan Li, Wei Xiang, Hui Xu, Bolong Lv, et al. Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat. Sci Discov. 2019;7(4):227-231. doi: 10.11648/j.sd.20190704.19

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@article{10.11648/j.sd.20190704.19,
  author = {Jie Li and Jianhuan Li and Wei Xiang and Hui Xu and Bolong Lv and Qing Wu},
  title = {Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat},
  journal = {Science Discovery},
  volume = {7},
  number = {4},
  pages = {227-231},
  doi = {10.11648/j.sd.20190704.19},
  url = {https://doi.org/10.11648/j.sd.20190704.19},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sd.20190704.19},
  abstract = {Aquatic animals are susceptible to N-dimethylnitrosamine pollution in water quality or feed, which is a non-negligible problem in food safety detection. Gas chromatography/triple four-stage mass spectrometry combined with QuEChERS was used to detect N-dimethylnitrosamine in duck and poultry meat, and acetonitrile, salting-out agent and purifying agent were used to extract duck and poultry meat samples. The results of detection and analysis showed that the results were good. The standard curve was highly correlated in the range of 5ng/mL to 1000ng/mL (R2 > 0.9997). The recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, instrument detection limit was 4.4ng/mL and method detection limit was 0.44ng/g after adding standard sample and matrix effect treatment. The results showed that the recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, and instrument detection limit was 4 ng/mL. Other methods can reduce the operation steps and improve the detection accuracy.},
 year = {2019}
}

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TY  - JOUR
T1  - Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat
AU  - Jie Li
AU  - Jianhuan Li
AU  - Wei Xiang
AU  - Hui Xu
AU  - Bolong Lv
AU  - Qing Wu
Y1  - 2019/08/27
PY  - 2019
N1  - https://doi.org/10.11648/j.sd.20190704.19
DO  - 10.11648/j.sd.20190704.19
T2  - Science Discovery
JF  - Science Discovery
JO  - Science Discovery
SP  - 227
EP  - 231
PB  - Science Publishing Group
SN  - 2331-0650
UR  - https://doi.org/10.11648/j.sd.20190704.19
AB  - Aquatic animals are susceptible to N-dimethylnitrosamine pollution in water quality or feed, which is a non-negligible problem in food safety detection. Gas chromatography/triple four-stage mass spectrometry combined with QuEChERS was used to detect N-dimethylnitrosamine in duck and poultry meat, and acetonitrile, salting-out agent and purifying agent were used to extract duck and poultry meat samples. The results of detection and analysis showed that the results were good. The standard curve was highly correlated in the range of 5ng/mL to 1000ng/mL (R2 > 0.9997). The recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, instrument detection limit was 4.4ng/mL and method detection limit was 0.44ng/g after adding standard sample and matrix effect treatment. The results showed that the recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, and instrument detection limit was 4 ng/mL. Other methods can reduce the operation steps and improve the detection accuracy.
VL  - 7
IS  - 4
ER  -

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Author Information

Jie Li

Anhui Topway Testing Service Co., Ltd., Xuancheng, China
Jianhuan Li

Anhui Topway Testing Service Co., Ltd., Xuancheng, China
Wei Xiang

Anhui Topway Testing Service Co., Ltd., Xuancheng, China
Hui Xu

Anhui Topway Testing Service Co., Ltd., Xuancheng, China
Bolong Lv

Anhui Topway Testing Service Co., Ltd., Xuancheng, China
Qing Wu

Anhui Topway Testing Service Co., Ltd., Xuancheng, China

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Sections

Plain Text BibTeX RIS

APA Style

Jie Li, Jianhuan Li, Wei Xiang, Hui Xu, Bolong Lv, et al. (2019). Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat. Science Discovery, 7(4), 227-231. https://doi.org/10.11648/j.sd.20190704.19

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ACS Style

Jie Li; Jianhuan Li; Wei Xiang; Hui Xu; Bolong Lv, et al. Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat. Sci. Discov. 2019, 7(4), 227-231. doi: 10.11648/j.sd.20190704.19

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AMA Style

Jie Li, Jianhuan Li, Wei Xiang, Hui Xu, Bolong Lv, et al. Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat. Sci Discov. 2019;7(4):227-231. doi: 10.11648/j.sd.20190704.19

Copy | Download

@article{10.11648/j.sd.20190704.19,
  author = {Jie Li and Jianhuan Li and Wei Xiang and Hui Xu and Bolong Lv and Qing Wu},
  title = {Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat},
  journal = {Science Discovery},
  volume = {7},
  number = {4},
  pages = {227-231},
  doi = {10.11648/j.sd.20190704.19},
  url = {https://doi.org/10.11648/j.sd.20190704.19},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sd.20190704.19},
  abstract = {Aquatic animals are susceptible to N-dimethylnitrosamine pollution in water quality or feed, which is a non-negligible problem in food safety detection. Gas chromatography/triple four-stage mass spectrometry combined with QuEChERS was used to detect N-dimethylnitrosamine in duck and poultry meat, and acetonitrile, salting-out agent and purifying agent were used to extract duck and poultry meat samples. The results of detection and analysis showed that the results were good. The standard curve was highly correlated in the range of 5ng/mL to 1000ng/mL (R2 > 0.9997). The recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, instrument detection limit was 4.4ng/mL and method detection limit was 0.44ng/g after adding standard sample and matrix effect treatment. The results showed that the recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, and instrument detection limit was 4 ng/mL. Other methods can reduce the operation steps and improve the detection accuracy.},
 year = {2019}
}

Copy | Download

TY  - JOUR
T1  - Study on Rapid Detection of N-Nitrosodimethylamine in Duck and Poultry Meat
AU  - Jie Li
AU  - Jianhuan Li
AU  - Wei Xiang
AU  - Hui Xu
AU  - Bolong Lv
AU  - Qing Wu
Y1  - 2019/08/27
PY  - 2019
N1  - https://doi.org/10.11648/j.sd.20190704.19
DO  - 10.11648/j.sd.20190704.19
T2  - Science Discovery
JF  - Science Discovery
JO  - Science Discovery
SP  - 227
EP  - 231
PB  - Science Publishing Group
SN  - 2331-0650
UR  - https://doi.org/10.11648/j.sd.20190704.19
AB  - Aquatic animals are susceptible to N-dimethylnitrosamine pollution in water quality or feed, which is a non-negligible problem in food safety detection. Gas chromatography/triple four-stage mass spectrometry combined with QuEChERS was used to detect N-dimethylnitrosamine in duck and poultry meat, and acetonitrile, salting-out agent and purifying agent were used to extract duck and poultry meat samples. The results of detection and analysis showed that the results were good. The standard curve was highly correlated in the range of 5ng/mL to 1000ng/mL (R2 > 0.9997). The recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, instrument detection limit was 4.4ng/mL and method detection limit was 0.44ng/g after adding standard sample and matrix effect treatment. The results showed that the recovery of standard sample was 82.51%-115.42%, RSD was 1.89-2.99, and instrument detection limit was 4 ng/mL. Other methods can reduce the operation steps and improve the detection accuracy.
VL  - 7
IS  - 4
ER  -

Copy | Download