Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer
Science Journal of Analytical Chemistry
Volume 4, Issue 3, May 2016, Pages: 22-25
Received: Mar. 19, 2016;
Accepted: Apr. 7, 2016;
Published: Apr. 27, 2016
Views 3595 Downloads 117
Y. Yildiz, Complete Analysis Laboratories, Analytical Research Department, Parsippany, NJ, USA
M. Dasgupta, Complete Analysis Laboratories, Analytical Research Department, Parsippany, NJ, USA
Follow on us
Tricalcium Phosphate Anhydrous Powder typically contains 300 to 400 mg/Kg (w/w) of aluminum. This level can be determined utilizing AAS and standard based on known standards. In this study, we have determined the amount of aluminum metal present in sample of Tricalcium Phosphate Anhydrous Powder using Atomic Absorption Spectrophotometer (AAS). The method has high precision and accuracy. The results of aluminum determinations obtained by employment of N2O-C2H2 flame AAS methods. Great care is necessary for preparation of the blank. The need to subtract blank with standard calibration curve this was done automatically. The accuracy was checked with recovery test of aluminum added to the sample before analysis. With employment of AAS method 98.5% and 99.0% of added aluminum was recovered. The detection limit for the determination of Al was 0.5 mg/Kg and results meet the requirements.
Tricalcium Phosphate, Aluminum Determination, Flame Atomic Absorption Spectrophotometer
To cite this article
Aluminum Determination for Tri-calcium Phosphate (TCP) Anhydrous Powder by Flame Atomic Absorption Spectrophotometer, Science Journal of Analytical Chemistry.
Vol. 4, No. 3,
2016, pp. 22-25.
Copyright © 2016 Authors retain the copyright of this article.
This article is an open access article distributed under the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/
) which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Ober, JA, Phosphate Rocks; U.S. Geological Survey Mineral Information.
Ahmed, M. J. and J. Hossan, 1995. Spectrophotometric determination of aluminum by morin. Talanta, 42(8): 1135-1142.
Huseyinli, A. A., R. Aliyeva, S. Haciyeva and T. Guray, 2009. Spectrophotometric determination of aluminum and indium with 2,2,3,4-tetrahydroxy-3,5-disulphoazobenzene. Journal of Hazardous Materials, 163: 1001-1007.
Francisco, B. A., L. S. Caldas, D. M. Brum and R. J. Cassella, 2010. Novel spectrophoto metricmethod for the determination of aluminum in soda drinks packed in cans and plastic bottles. Journal of Hazardous Materials, 181: 485-490.
Honorato, R. S., J. M. T. Carnerio and E. A. G. Zagatto, 2001. Spectrophotometric flow-batch determination of aluminum in plant tissues exploiting a feedback mechanism. Analytical Chimica Acta, 441:309-315.
Bulut, V. N., D. Arslan, D. Ozdes, M. Soylak and M. Tufekci, 2010. Preconcentration, separation and spectrophotometric determination of aluminum (III) in water samples and dialysis concentrates at trace levels with 8-hydroxyquinoline-cobalt(II) coprecipitation system. 182: 331-336.
Burguera, J. L., M. Burguera, C. Rondon, P. Carrero, M. R. Brunetto and Y. Petitde Pena, 2000. Determination of beryllium in natural and waste waters using on-line flow-injection preconcentration by precipitation: dissolution for electrothermal atomic absorption spectrometry. Talanta, 52: 27-37.