Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar

Qiang Sun; Yuliang Gao; Liyan Wang

doi:doi:10.11648/j.sjac.20200801.12

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Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar

Qiang Sun, Yuliang Gao, Liyan Wang

Published in Science Journal of Analytical Chemistry (Volume 8, Issue 1)

Received: 21 December 2019 Accepted: 8 January 2020 Published: 31 January 2020

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Abstract

A simple, efficient and environmentally friendly method has been established for the analysis of organic components in wood vinegar (WV) by dispersive liquid-liquid micro-extraction based on solidification of floating organic droplet (DLLME-SFO) coupled with GC/MS. Several variables that affect the extraction efficiency, including the type and volume of the extractant and dispersant, extraction time and the mass fraction of sodium chloride were optimized. Under the optimum conditions, the sample extracted were analyzed by GC/MS. The result shows that, apart from the main component of acetic acid, many kinds of ketone compound, phenol compound, ester compound, aldehyde and alcohol compound exist in the WV. The proposed method has been successfully employed to determine the organic components in the WV.

Published in	Science Journal of Analytical Chemistry (Volume 8, Issue 1)
DOI	10.11648/j.sjac.20200801.12
Page(s)	5-11
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Wood Vinegar, DLLME-SFO, GC/MS, Organic Components

References

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APA Style

Qiang Sun, Yuliang Gao, Liyan Wang. (2020). Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar. Science Journal of Analytical Chemistry, 8(1), 5-11. https://doi.org/10.11648/j.sjac.20200801.12

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ACS Style

Qiang Sun; Yuliang Gao; Liyan Wang. Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar. Sci. J. Anal. Chem. 2020, 8(1), 5-11. doi: 10.11648/j.sjac.20200801.12

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AMA Style

Qiang Sun, Yuliang Gao, Liyan Wang. Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar. Sci J Anal Chem. 2020;8(1):5-11. doi: 10.11648/j.sjac.20200801.12

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@article{10.11648/j.sjac.20200801.12,
  author = {Qiang Sun and Yuliang Gao and Liyan Wang},
  title = {Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar},
  journal = {Science Journal of Analytical Chemistry},
  volume = {8},
  number = {1},
  pages = {5-11},
  doi = {10.11648/j.sjac.20200801.12},
  url = {https://doi.org/10.11648/j.sjac.20200801.12},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sjac.20200801.12},
  abstract = {A simple, efficient and environmentally friendly method has been established for the analysis of organic components in wood vinegar (WV) by dispersive liquid-liquid micro-extraction based on solidification of floating organic droplet (DLLME-SFO) coupled with GC/MS. Several variables that affect the extraction efficiency, including the type and volume of the extractant and dispersant, extraction time and the mass fraction of sodium chloride were optimized. Under the optimum conditions, the sample extracted were analyzed by GC/MS. The result shows that, apart from the main component of acetic acid, many kinds of ketone compound, phenol compound, ester compound, aldehyde and alcohol compound exist in the WV. The proposed method has been successfully employed to determine the organic components in the WV.},
 year = {2020}
}

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TY  - JOUR
T1  - Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar
AU  - Qiang Sun
AU  - Yuliang Gao
AU  - Liyan Wang
Y1  - 2020/01/31
PY  - 2020
N1  - https://doi.org/10.11648/j.sjac.20200801.12
DO  - 10.11648/j.sjac.20200801.12
T2  - Science Journal of Analytical Chemistry
JF  - Science Journal of Analytical Chemistry
JO  - Science Journal of Analytical Chemistry
SP  - 5
EP  - 11
PB  - Science Publishing Group
SN  - 2376-8053
UR  - https://doi.org/10.11648/j.sjac.20200801.12
AB  - A simple, efficient and environmentally friendly method has been established for the analysis of organic components in wood vinegar (WV) by dispersive liquid-liquid micro-extraction based on solidification of floating organic droplet (DLLME-SFO) coupled with GC/MS. Several variables that affect the extraction efficiency, including the type and volume of the extractant and dispersant, extraction time and the mass fraction of sodium chloride were optimized. Under the optimum conditions, the sample extracted were analyzed by GC/MS. The result shows that, apart from the main component of acetic acid, many kinds of ketone compound, phenol compound, ester compound, aldehyde and alcohol compound exist in the WV. The proposed method has been successfully employed to determine the organic components in the WV.
VL  - 8
IS  - 1
ER  -

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Author Information

Qiang Sun

Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China
Yuliang Gao

Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China
Liyan Wang

Agonomy College, Heilongjiang Bayi Agricultural University, Daqing, China

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Plain Text BibTeX RIS

APA Style

Qiang Sun, Yuliang Gao, Liyan Wang. (2020). Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar. Science Journal of Analytical Chemistry, 8(1), 5-11. https://doi.org/10.11648/j.sjac.20200801.12

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ACS Style

Qiang Sun; Yuliang Gao; Liyan Wang. Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar. Sci. J. Anal. Chem. 2020, 8(1), 5-11. doi: 10.11648/j.sjac.20200801.12

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AMA Style

Qiang Sun, Yuliang Gao, Liyan Wang. Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar. Sci J Anal Chem. 2020;8(1):5-11. doi: 10.11648/j.sjac.20200801.12

Copy | Download

@article{10.11648/j.sjac.20200801.12,
  author = {Qiang Sun and Yuliang Gao and Liyan Wang},
  title = {Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar},
  journal = {Science Journal of Analytical Chemistry},
  volume = {8},
  number = {1},
  pages = {5-11},
  doi = {10.11648/j.sjac.20200801.12},
  url = {https://doi.org/10.11648/j.sjac.20200801.12},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.sjac.20200801.12},
  abstract = {A simple, efficient and environmentally friendly method has been established for the analysis of organic components in wood vinegar (WV) by dispersive liquid-liquid micro-extraction based on solidification of floating organic droplet (DLLME-SFO) coupled with GC/MS. Several variables that affect the extraction efficiency, including the type and volume of the extractant and dispersant, extraction time and the mass fraction of sodium chloride were optimized. Under the optimum conditions, the sample extracted were analyzed by GC/MS. The result shows that, apart from the main component of acetic acid, many kinds of ketone compound, phenol compound, ester compound, aldehyde and alcohol compound exist in the WV. The proposed method has been successfully employed to determine the organic components in the WV.},
 year = {2020}
}

Copy | Download

TY  - JOUR
T1  - Analysis of Organic Components by DLLME Based on the Solidification of a Floating Organic Droplet Followed with GC/MS in Wood Vinegar
AU  - Qiang Sun
AU  - Yuliang Gao
AU  - Liyan Wang
Y1  - 2020/01/31
PY  - 2020
N1  - https://doi.org/10.11648/j.sjac.20200801.12
DO  - 10.11648/j.sjac.20200801.12
T2  - Science Journal of Analytical Chemistry
JF  - Science Journal of Analytical Chemistry
JO  - Science Journal of Analytical Chemistry
SP  - 5
EP  - 11
PB  - Science Publishing Group
SN  - 2376-8053
UR  - https://doi.org/10.11648/j.sjac.20200801.12
AB  - A simple, efficient and environmentally friendly method has been established for the analysis of organic components in wood vinegar (WV) by dispersive liquid-liquid micro-extraction based on solidification of floating organic droplet (DLLME-SFO) coupled with GC/MS. Several variables that affect the extraction efficiency, including the type and volume of the extractant and dispersant, extraction time and the mass fraction of sodium chloride were optimized. Under the optimum conditions, the sample extracted were analyzed by GC/MS. The result shows that, apart from the main component of acetic acid, many kinds of ketone compound, phenol compound, ester compound, aldehyde and alcohol compound exist in the WV. The proposed method has been successfully employed to determine the organic components in the WV.
VL  - 8
IS  - 1
ER  -

Copy | Download