GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from <i>Cinnamomum culilawan</i>, Blume

Hanoch Julianus Sohilait; Healthy Kainama

doi:doi:10.11648/j.ajac.20160404.16

| Peer-Reviewed

GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume

Hanoch Julianus Sohilait, Healthy Kainama

Published in American Journal of Applied Chemistry (Volume 4, Issue 4)

Received: 1 July 2016 Accepted: 13 July 2016 Published: 2 August 2016

Views: Downloads:

Download PDF

Share This Article

Twitter
Linked In
Facebook

Abstract

The essentials oils (EO) in Cinnamomum culilawan bark have been isolated by steam distillation and evaluated by GC/GC-MS, IR and NMR methods. The GC/GC-MS analysis identified 12 compounds. The major components are eugenol (66.477%), safrole (12.432%) and methyleugenol (6.972%). Repeated purification of the two main compounds yielded eugenol (51.66%), and safrole (6.71%).

Published in	American Journal of Applied Chemistry (Volume 4, Issue 4)
DOI	10.11648/j.ajac.20160404.16
Page(s)	157-160
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Cinnamomum culilawan, Bark Essential Oil, Chemical Composition, Eugenol, Safrole

References

[1]	Ketaren S, Pengantar Minyak Atsiri, PN. Balai Pustaka, Jakarta, 1985.
[2]	Sastrohamidjojo H, Kimia Minyak Atsiri, Gadjah Mada University Press, 2004.
[3]	LenseO, The wild plants used as traditional medicines by indigenous people of Manokwari, West Papua, Bio Diversitas, 2012, 13 (2), 98-106.
[4]	Jantan I, Ali N. A. M, Ahmad A. R and Ahmad A. S, Chemical constituents of the essential oils of Cinnamomum sintoc, Blume, Pertanika J. Sci. & Techno., 1994, 2 (1), 39-45.
[5]	Iskandar Y, Supriyatna S, Chemical composition of volatile oil from Cinnamomum sintoc stem barks, Proceeding of The international seminar on chemistry, Jatinangor, Indonesia, 2008, 601-603
[6]	Reynertson K. A, Balick M. J, Lee R, Raynor W, Pelep Y, Kennelly E. J, A traditional method of Cinnamomum carolinense preparation eliminates safrole from a therapeutic Pohnpean tea, J. Ethnopharmacology, 2005, 102, 269–274.
[7]	Luo Y, LuoYo, Chen F, Liu H, Studies on the Chemical constituents in the essential oils from the leaves of Cinnamomum bodinieri Levi, Adv. Meterials Res., 2014, 1015, 373-376.
[8]	Kapelle I. B. D, Irawadi, T. T, Rusli M. S, Mangunwidjaja D, Mas’ud, Z. A, Synthesis of new curcumin analogues from kulitlawang oils using the conventional method and microwave, Sci. J. Chem., 2015, 3 (3): 50-56.
[9]	Sohilait M. R, Sohilait, H. J, Fransina E, 2013, Synthesis of 34-methylenedioxy isoamylcinamic as the sunscreen Compound from culilawang oil, Ind. J. Chem. Res., 2013, 1, 1-5.
[10]	Li H. Q, Liu Q. Z, Liu Z. L, Du Sh. Sh and Deng Z. W, Chemical composition and nematicidalactivity of essential oil of Agastacherugosaagainst Meloidogyne incognita, Molecules, 2013, 18, 4170-4180.
[11]	Chu S. S, Cheng Fang Wang C. F, Du S. S, Liu S. L, Liu Z. L, Toxicity of the essential oil of Illiciumdifengpistem bark and its constituent compounds towards two grain storage insects, J. Insect Sci., 2011, 11 (152), 1-10.
[12]	Valente V. M. M, Jham G. N, Jardim C. M, Dhingra O. D, Ghiviriga I, Major antifungals in nutmeg essential oil against Aspergillus flavus and A. ochraceus, J. Food Res., 2015, 4 (1), 51-57.
[13]	Kamatou G. P, Vermaak I and Viljoen A. M, Eugenol- From the remote Maluku Islands to the international market place: A review of a remarkable and versatile molecule, Molecules, 2012, 17, 6953-6981.
[14]	Huang Y, Ho S. H, Lee H. C, Yap Y. L. Insecticidal properties of eugenol, isoeugenol and methyleugenol and their effectson nutrition of Sitophilus zeamais Motsch. (Coleoptera: Curculionidae) and Tribolium castaneum (Herbst) (Coleoptera: Tenebrionidae), J. Stored Prod. Res., 2002, 38, 403-412.
[15]	Ozturk A, Ozbek H, The Anti-inflammatory activity of Eugenia caryophyllata essential oil: An animal model of anti-inflammatory activity, Eur. J. Gen. Med., 2005, 2 (4), 159-163.

Cite This Article

Plain Text BibTeX RIS

APA Style

Hanoch Julianus Sohilait, Healthy Kainama. (2016). GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume. American Journal of Applied Chemistry, 4(4), 157-160. https://doi.org/10.11648/j.ajac.20160404.16

Copy | Download

ACS Style

Hanoch Julianus Sohilait; Healthy Kainama. GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume. Am. J. Appl. Chem. 2016, 4(4), 157-160. doi: 10.11648/j.ajac.20160404.16

Copy | Download

AMA Style

Hanoch Julianus Sohilait, Healthy Kainama. GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume. Am J Appl Chem. 2016;4(4):157-160. doi: 10.11648/j.ajac.20160404.16

Copy | Download

@article{10.11648/j.ajac.20160404.16,
  author = {Hanoch Julianus Sohilait and Healthy Kainama},
  title = {GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume},
  journal = {American Journal of Applied Chemistry},
  volume = {4},
  number = {4},
  pages = {157-160},
  doi = {10.11648/j.ajac.20160404.16},
  url = {https://doi.org/10.11648/j.ajac.20160404.16},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajac.20160404.16},
  abstract = {The essentials oils (EO) in Cinnamomum culilawan bark have been isolated by steam distillation and evaluated by GC/GC-MS, IR and NMR methods. The GC/GC-MS analysis identified 12 compounds. The major components are eugenol (66.477%), safrole (12.432%) and methyleugenol (6.972%). Repeated purification of the two main compounds yielded eugenol (51.66%), and safrole (6.71%).},
 year = {2016}
}

Copy | Download

TY  - JOUR
T1  - GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume
AU  - Hanoch Julianus Sohilait
AU  - Healthy Kainama
Y1  - 2016/08/02
PY  - 2016
N1  - https://doi.org/10.11648/j.ajac.20160404.16
DO  - 10.11648/j.ajac.20160404.16
T2  - American Journal of Applied Chemistry
JF  - American Journal of Applied Chemistry
JO  - American Journal of Applied Chemistry
SP  - 157
EP  - 160
PB  - Science Publishing Group
SN  - 2330-8745
UR  - https://doi.org/10.11648/j.ajac.20160404.16
AB  - The essentials oils (EO) in Cinnamomum culilawan bark have been isolated by steam distillation and evaluated by GC/GC-MS, IR and NMR methods. The GC/GC-MS analysis identified 12 compounds. The major components are eugenol (66.477%), safrole (12.432%) and methyleugenol (6.972%). Repeated purification of the two main compounds yielded eugenol (51.66%), and safrole (6.71%).
VL  - 4
IS  - 4
ER  -

Copy | Download

Author Information

Hanoch Julianus Sohilait

Departement of Chemistry, Faculty of Mathematic and Natural Science, Pattimura University, Ambon, Indonesia
Healthy Kainama

Departement of Chemistry Education, Faculty of Training and Education, Pattimura University, Ambon, Indonesia

Download PDF

Sections

Plain Text BibTeX RIS

APA Style

Hanoch Julianus Sohilait, Healthy Kainama. (2016). GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume. American Journal of Applied Chemistry, 4(4), 157-160. https://doi.org/10.11648/j.ajac.20160404.16

Copy | Download

ACS Style

Hanoch Julianus Sohilait; Healthy Kainama. GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume. Am. J. Appl. Chem. 2016, 4(4), 157-160. doi: 10.11648/j.ajac.20160404.16

Copy | Download

AMA Style

Hanoch Julianus Sohilait, Healthy Kainama. GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume. Am J Appl Chem. 2016;4(4):157-160. doi: 10.11648/j.ajac.20160404.16

Copy | Download

@article{10.11648/j.ajac.20160404.16,
  author = {Hanoch Julianus Sohilait and Healthy Kainama},
  title = {GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume},
  journal = {American Journal of Applied Chemistry},
  volume = {4},
  number = {4},
  pages = {157-160},
  doi = {10.11648/j.ajac.20160404.16},
  url = {https://doi.org/10.11648/j.ajac.20160404.16},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ajac.20160404.16},
  abstract = {The essentials oils (EO) in Cinnamomum culilawan bark have been isolated by steam distillation and evaluated by GC/GC-MS, IR and NMR methods. The GC/GC-MS analysis identified 12 compounds. The major components are eugenol (66.477%), safrole (12.432%) and methyleugenol (6.972%). Repeated purification of the two main compounds yielded eugenol (51.66%), and safrole (6.71%).},
 year = {2016}
}

Copy | Download

TY  - JOUR
T1  - GC/GC-MS Analysis, Isolation and Identification of Bark Essential Oil Components from Cinnamomum culilawan, Blume
AU  - Hanoch Julianus Sohilait
AU  - Healthy Kainama
Y1  - 2016/08/02
PY  - 2016
N1  - https://doi.org/10.11648/j.ajac.20160404.16
DO  - 10.11648/j.ajac.20160404.16
T2  - American Journal of Applied Chemistry
JF  - American Journal of Applied Chemistry
JO  - American Journal of Applied Chemistry
SP  - 157
EP  - 160
PB  - Science Publishing Group
SN  - 2330-8745
UR  - https://doi.org/10.11648/j.ajac.20160404.16
AB  - The essentials oils (EO) in Cinnamomum culilawan bark have been isolated by steam distillation and evaluated by GC/GC-MS, IR and NMR methods. The GC/GC-MS analysis identified 12 compounds. The major components are eugenol (66.477%), safrole (12.432%) and methyleugenol (6.972%). Repeated purification of the two main compounds yielded eugenol (51.66%), and safrole (6.71%).
VL  - 4
IS  - 4
ER  -

Copy | Download