Synthesis, Spectroscopic Characterization and Powder XRD Study of 4-(5-(Ethylthio)-1,3,4-Oxadiazole-2-yl) Aniline
American Journal of Applied Chemistry
Volume 3, Issue 5-1, October 2015, Pages: 1-6
Received: Nov. 25, 2014; Accepted: Nov. 27, 2014; Published: Dec. 27, 2014
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Authors
Emad Ghanem, Department of Chemistry, Faculty of Sciences, Damascus University, Damascus, Syrian Arab Republic
Sahar Al-Hariri, Department of Chemistry, Faculty of Sciences, Damascus University, Damascus, Syrian Arab Republic
Abeer Ghanem, Higher Institute of Laser Research, Damascus University, Damascus, Syrian Arab Republic
Lama Aouda, Higher Institute of Laser Research, Damascus University, Damascus, Syrian Arab Republic
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Abstract
In order to investigate the separation mechanism of liquid crystals stationary phases based on an oxadiazole moiety, new 1,3,4-oxadiazole derivative as side mesogenic arm in liquid crystals was prepared, and its structural spectroscopic data were studied in this paper. A powerful indication about the relationship between molecular structure and alignment properties is described. Such information is indispensable for the design and synthesis new liquid crystals stationary phases of high separation efficiency.
Keywords
Oxadiazole, Liquid Crystal, Characterization, XRD, Synthesis
To cite this article
Emad Ghanem, Sahar Al-Hariri, Abeer Ghanem, Lama Aouda, Synthesis, Spectroscopic Characterization and Powder XRD Study of 4-(5-(Ethylthio)-1,3,4-Oxadiazole-2-yl) Aniline, American Journal of Applied Chemistry. Special Issue: Development of Liquid Crystalline Stationary Phases for Liquid and Gas Chromatographic Separations. Vol. 3, No. 5-1, 2015, pp. 1-6. doi: 10.11648/j.ajac.s.2015030501.11
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