International Journal of Pharmacy and Chemistry

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A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples

Received: 16 September 2020    Accepted: 30 September 2020    Published: 11 November 2020
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Abstract

The pesticide residues in foods have received increasing attention as one of the most important food safety issues. Therefore, more strict regulations on the maximum residue limits (MRLs) for pesticides in foods have been established in many countries and health organizations, based on the sensitive and reliable analysis methods of pesticide residues. However, the analysis of pesticide residues is a continuing challenge mainly because of the small quantities of analytes as well as the large amounts of interfering substances which can be co-extracted with them, often leading to experimental errors and damage to the Analytical instruments. Thus, extensive sample preparation is often required for the pesticide residue analysis for the effective extraction of the analytes and removal of the interferences. This paper focuses on reviewing the recent development in the sample preparation methods for the pesticide residue analysis in some food samples. The methods include: Liquid-Liquid extraction (LLE), Solid-Phase extraction (SPE), Matrix Solid-Phase Dispersion (MSPD), Solid-Phase Micro-extraction (SPME), QuEChERS, and Liquid Phase Micro-extraction (LPME).

DOI 10.11648/j.ijpc.20200606.11
Published in International Journal of Pharmacy and Chemistry (Volume 6, Issue 6, November 2020)
Page(s) 65-76
Creative Commons

This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Sample Preparation, Pesticide Residues, Food, Extraction, Clean-up

References
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  • Department of Chemistry, Oda Bultum University, Chiro, Ethiopia

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    Shibiru Eticha. (2020). A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. International Journal of Pharmacy and Chemistry, 6(6), 65-76. https://doi.org/10.11648/j.ijpc.20200606.11

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    Shibiru Eticha. A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. Int. J. Pharm. Chem. 2020, 6(6), 65-76. doi: 10.11648/j.ijpc.20200606.11

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    AMA Style

    Shibiru Eticha. A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples. Int J Pharm Chem. 2020;6(6):65-76. doi: 10.11648/j.ijpc.20200606.11

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  • @article{10.11648/j.ijpc.20200606.11,
      author = {Shibiru Eticha},
      title = {A Review: Sample Preparation Methods for the Pesticide Residue Analysis in Food Samples},
      journal = {International Journal of Pharmacy and Chemistry},
      volume = {6},
      number = {6},
      pages = {65-76},
      doi = {10.11648/j.ijpc.20200606.11},
      url = {https://doi.org/10.11648/j.ijpc.20200606.11},
      eprint = {https://download.sciencepg.com/pdf/10.11648.j.ijpc.20200606.11},
      abstract = {The pesticide residues in foods have received increasing attention as one of the most important food safety issues. Therefore, more strict regulations on the maximum residue limits (MRLs) for pesticides in foods have been established in many countries and health organizations, based on the sensitive and reliable analysis methods of pesticide residues. However, the analysis of pesticide residues is a continuing challenge mainly because of the small quantities of analytes as well as the large amounts of interfering substances which can be co-extracted with them, often leading to experimental errors and damage to the Analytical instruments. Thus, extensive sample preparation is often required for the pesticide residue analysis for the effective extraction of the analytes and removal of the interferences. This paper focuses on reviewing the recent development in the sample preparation methods for the pesticide residue analysis in some food samples. The methods include: Liquid-Liquid extraction (LLE), Solid-Phase extraction (SPE), Matrix Solid-Phase Dispersion (MSPD), Solid-Phase Micro-extraction (SPME), QuEChERS, and Liquid Phase Micro-extraction (LPME).},
     year = {2020}
    }
    

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    AB  - The pesticide residues in foods have received increasing attention as one of the most important food safety issues. Therefore, more strict regulations on the maximum residue limits (MRLs) for pesticides in foods have been established in many countries and health organizations, based on the sensitive and reliable analysis methods of pesticide residues. However, the analysis of pesticide residues is a continuing challenge mainly because of the small quantities of analytes as well as the large amounts of interfering substances which can be co-extracted with them, often leading to experimental errors and damage to the Analytical instruments. Thus, extensive sample preparation is often required for the pesticide residue analysis for the effective extraction of the analytes and removal of the interferences. This paper focuses on reviewing the recent development in the sample preparation methods for the pesticide residue analysis in some food samples. The methods include: Liquid-Liquid extraction (LLE), Solid-Phase extraction (SPE), Matrix Solid-Phase Dispersion (MSPD), Solid-Phase Micro-extraction (SPME), QuEChERS, and Liquid Phase Micro-extraction (LPME).
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