American Journal of Applied Chemistry

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Synthesis and Investigation of Polyester and Poly Amide Azo Dyes (I)

Received: 17 December 2014    Accepted: 25 December 2014    Published: 20 January 2015
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Abstract

The preparation of monomer dyes was carried out by formation of diazinium salt of amine compound to coupled with Ρ- toluidine, aniline to form azo dyes with function (hydroxy and amino) groups. the polymerized was carried out with different diacid chloride or modified with acroyl chloride to polymerize with methylmethacrylate (MMA) by two method solution and interfacial poly condensation methods, the prepared mono azodye, poly(ester) and poly(amide) azopolymers were characterized, by infrared spectroscopy, elemental analysis, 1H NMR, thermodynamic (TGA), thermo gravimetric (DSC) analysis and TGA. The molecular weights were measured by GPC. The synthesized polymers showed a good film forming properties.

DOI 10.11648/j.ajac.20150301.12
Published in American Journal of Applied Chemistry (Volume 3, Issue 1, February 2015)
Page(s) 6-13
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This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.

Copyright

Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Azo Polymers, Polyesters and Polyamides

References
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[2] Yin S, Xu H, shi W ,Gao y, Song Y and Wing J, Polymer, 2005,46,7670.
[3] Nabeshima Y, Shishido A, Kanazawa A, Shiono T, Ikeda t and Hiyama T, Chem Mater1997, 9, 1480.
[4] Hallas G and Towns A D, Dyes pigments, 1997, 33,319.
[5] Towns A D, Dyes pigments, 1999, 42, 3.
[6] T. Mandel., and Y. Inber., Chem. Phys. Lett. 2004, 165, 387.
[7] Hasanain A S. A Majeed, Alaa Yassin Al-Ahmad and Kawkab Ali Hussain, The Preparation, Characterization and the Study of the Linear Optical Properties of a New Azo Compound, Journal of Basrah Researches ((Sciences)) 2011,Vol.37.No. 2,.
[8] E. Saion, Susilawati, A.Doyan,S. Zainal, Z. Azmi, A. Zulkfi, A.R.MohdZaki,K.Z.H. Dahlan and T.Karni, "Changes in the Optical Band Gap and ν Absorption Edge of Gamma-Irradiated Polymer Blends “,J. Appl. Sci." , 2005, 5, 10, 1825-1829.
[9] Gardziella,A. Pilao, L.A., and Know, A., Phenolic Resins: chemistry, Applications,standardization, safety and Ecology, 2000,New York: springer.
[10] Giles C H , A Laboratory Course in Dyeing , 3rd ed ( Socity of Dyers and Colorist , Bradford ) 1974
[11] W, Jie-xiong et al. Application of Polymeric Dyes in Textile Fields, Application of Polymeric Dyes in Textile Fields, The Proceedings of the 3rd International Conference on Functional Molecules
Author Information
  • Health science program, Biology Department, Faculty of Science, King Khalid University, Women center Al-Samer, Abha, KSA; Health science program, King Khalid University, P.O. 3340, Saudi Arabia

  • Health science program, Biology Department, Faculty of Science, King Khalid University, Women center Al-Samer, Abha, KSA

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    Rehab Abdeen, H. O. BadrEldin. (2015). Synthesis and Investigation of Polyester and Poly Amide Azo Dyes (I). American Journal of Applied Chemistry, 3(1), 6-13. https://doi.org/10.11648/j.ajac.20150301.12

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    Rehab Abdeen; H. O. BadrEldin. Synthesis and Investigation of Polyester and Poly Amide Azo Dyes (I). Am. J. Appl. Chem. 2015, 3(1), 6-13. doi: 10.11648/j.ajac.20150301.12

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    AMA Style

    Rehab Abdeen, H. O. BadrEldin. Synthesis and Investigation of Polyester and Poly Amide Azo Dyes (I). Am J Appl Chem. 2015;3(1):6-13. doi: 10.11648/j.ajac.20150301.12

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  • @article{10.11648/j.ajac.20150301.12,
      author = {Rehab Abdeen and H. O. BadrEldin},
      title = {Synthesis and Investigation of Polyester and Poly Amide Azo Dyes (I)},
      journal = {American Journal of Applied Chemistry},
      volume = {3},
      number = {1},
      pages = {6-13},
      doi = {10.11648/j.ajac.20150301.12},
      url = {https://doi.org/10.11648/j.ajac.20150301.12},
      eprint = {https://download.sciencepg.com/pdf/10.11648.j.ajac.20150301.12},
      abstract = {The preparation of monomer dyes was carried out by formation of diazinium salt of amine compound to coupled with Ρ- toluidine, aniline to form azo dyes with function (hydroxy and amino) groups. the polymerized was carried out with different diacid chloride or modified with acroyl chloride to polymerize with methylmethacrylate (MMA) by two method solution and interfacial poly condensation methods, the prepared mono azodye, poly(ester) and poly(amide) azopolymers were characterized, by infrared spectroscopy, elemental analysis, 1H NMR, thermodynamic (TGA), thermo gravimetric (DSC) analysis and TGA. The molecular weights were measured by GPC. The synthesized polymers showed a good film forming properties.},
     year = {2015}
    }
    

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    T1  - Synthesis and Investigation of Polyester and Poly Amide Azo Dyes (I)
    AU  - Rehab Abdeen
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    AB  - The preparation of monomer dyes was carried out by formation of diazinium salt of amine compound to coupled with Ρ- toluidine, aniline to form azo dyes with function (hydroxy and amino) groups. the polymerized was carried out with different diacid chloride or modified with acroyl chloride to polymerize with methylmethacrylate (MMA) by two method solution and interfacial poly condensation methods, the prepared mono azodye, poly(ester) and poly(amide) azopolymers were characterized, by infrared spectroscopy, elemental analysis, 1H NMR, thermodynamic (TGA), thermo gravimetric (DSC) analysis and TGA. The molecular weights were measured by GPC. The synthesized polymers showed a good film forming properties.
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